Information card for entry 7108665

Structure parameters

• Formula: C35 H50 Cl7 N4 O4 Rh2
• Calculated formula: C35 H50 Cl7 N4 O4 Rh2
• Title of publication: Introducing a mixed-valent dirhodium(II,III) catalyst with increased stability in C-H amination
• Authors of publication: Katherine P. Kornecki; John F. Berry
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 12097
• a: 12.6948 ± 0.0006 Å
• b: 13.6859 ± 0.0006 Å
• c: 14.8577 ± 0.0007 Å
• α: 71.541 ± 0.003°
• β: 65.929 ± 0.002°
• γ: 66.835 ± 0.003°
• Cell volume: 2129.04 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0863
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.1643
• Weighted residual factors for all reflections included in the refinement: 0.1857
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No