Information card for entry 7108677

Structure parameters

• Formula: C38 H68 Cl2 Ge N2 O P2
• Calculated formula: C38 H68 Cl2 Ge N2 O P2
• Title of publication: Germyliumylidene [ClGe:]+and Germathionium [ClGe=S]+ Supported by 1,8-bis(Tributylphosphazenyl)naphthalene
• Authors of publication: Matthias Driess; Yun Xiong; Shenglai Yao; Andreas Berkefeld; Shigeyoshi Inoue
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 12198
• a: 12.4821 ± 0.0007 Å
• b: 19.3868 ± 0.0008 Å
• c: 19.0651 ± 0.0012 Å
• α: 90°
• β: 103.496 ± 0.006°
• γ: 90°
• Cell volume: 4486.1 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0606
• Weighted residual factors for significantly intense reflections: 0.1229
• Weighted residual factors for all reflections included in the refinement: 0.1325
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No