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Information card for entry 7108726
Preview
Coordinates | 7108726.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C17 H24 O2 Si |
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Calculated formula | C17 H24 O2 Si |
SMILES | [Si](C1=C2CC[C@H]3OC[C@@H]4CCC(=C(C1=O)[C@]234)C)(C)(C)C |
Title of publication | A quick access to the spirotricyclic core analogue of mangicol A by a Rh(I)-catalyzed tandem Pauson-Khand/[4+2] cycloaddition |
Authors of publication | Wei Chen; Jia-Hui Tay; Jun Ying; Michal Sabat; Xiao-Qi Yu; Lin Pu |
Journal of publication | Chem.Commun. |
Year of publication | 2013 |
Journal volume | 49 |
Pages of publication | 170 |
a | 9.1005 ± 0.0003 Å |
b | 12.8251 ± 0.0005 Å |
c | 13.4859 ± 0.0005 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1574 ± 0.1 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0308 |
Residual factor for significantly intense reflections | 0.0283 |
Weighted residual factors for significantly intense reflections | 0.0955 |
Weighted residual factors for all reflections included in the refinement | 0.1 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.874 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7108726.html
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