Information card for entry 7108736

Structure parameters

• Formula: C128 Ag6 N8 O72 Si2 W20
• Calculated formula: C128.3 Ag6 N8 O72 Si2 W20
• Title of publication: A discrete octahedrally shaped [Ag6]^4+^ cluster encapsulated within silicotungstate ligands
• Authors of publication: Yuji Kikukawa; Yoshiyuki Kuroda; Kosuke Suzuki; Mitsuhiro Hibino; Kazuya Yamaguchi; Noritaka Mizuno
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 376
• a: 22.3265 ± 0.0002 Å
• b: 18.8039 ± 0.0003 Å
• c: 27.4531 ± 0.0004 Å
• α: 90°
• β: 94.39°
• γ: 90°
• Cell volume: 11491.7 ± 0.3 ų
• Cell temperature: 153 K
• Ambient diffraction temperature: 153 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0864
• Weighted residual factors for all reflections included in the refinement: 0.2753
• Goodness-of-fit parameter for all reflections included in the refinement: 1.107
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No