Information card for entry 7108804

Structure parameters

• Formula: C52 H40 Ag2 Cl6 N4 O6
• Calculated formula: C52 H40 Ag2 Cl5.998 N4 O5.994
• Title of publication: Single-crystal-to-single-crystal direct cross-linking and photopolymerisation of a discrete Ag(I) complex to give a 1D polycyclobutane coordination polymer
• Authors of publication: Saikat Dutta; Dejan-Kresimir Bucar; Elizabeth Elacqua; Leonard R. MacGillivray
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2013
• Journal volume: 49
• Journal issue: 11
• Pages of publication: 1064 - 1066
• a: 8.9589 ± 0.001 Å
• b: 11.5427 ± 0.0013 Å
• c: 13.4841 ± 0.0014 Å
• α: 97.692 ± 0.007°
• β: 102.484 ± 0.006°
• γ: 103.767 ± 0.005°
• Cell volume: 1296.8 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1153
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.1616
• Weighted residual factors for all reflections included in the refinement: 0.1801
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No