Information card for entry 7108993

Structure parameters

• Formula: C31 H81 K O3 Si10
• Calculated formula: C31 H81 K O3 Si10
• SMILES: [Si]1([Si]([Si]([Si]([Si]1([Si](C)(C)C)[Si](C)(C)C)(C)C)(C)C)([Si](C)(C)C)[Si](C)(C)C)([Si](C)(C)C)[K]([O]1CCCC1)([O]1CCCC1)[O]1CCCC1
• Title of publication: Reduction of the dihalocyclopentasilanes. A quest for a homocyclic silylene
• Authors of publication: Xu-Qiong Xiao; Hui Zhao; Zheng Xu; Guoqiao Lai; Xiao-Lin He; Zhifang Li
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 2706
• a: 10.925 ± 0.003 Å
• b: 25.574 ± 0.007 Å
• c: 18.928 ± 0.005 Å
• α: 90°
• β: 96.712 ± 0.005°
• γ: 90°
• Cell volume: 5252 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.121
• Residual factor for significantly intense reflections: 0.0625
• Weighted residual factors for significantly intense reflections: 0.1574
• Weighted residual factors for all reflections included in the refinement: 0.1892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No