Information card for entry 7109022

Structure parameters

• Formula: C24 H46 B Co F4 N P2
• Calculated formula: C24 H46 B Co F4 N P2
• Title of publication: Formal loss of an H radical by a cobalt complex via metal-ligand cooperation
• Authors of publication: Eugene Khaskin; Yael Diskin-Posner; Lev Weiner; Gregory Leitus; David Milstein
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 2771
• a: 8.3331 ± 0.0003 Å
• b: 12.3139 ± 0.0005 Å
• c: 14.4758 ± 0.0005 Å
• α: 73.052 ± 0.002°
• β: 76.271 ± 0.002°
• γ: 88.469 ± 0.003°
• Cell volume: 1378.85 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0504
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0818
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No