Information card for entry 7109037

Structure parameters

• Formula: C29 H41 N4 O5
• Calculated formula: C29 H41 N4 O5
• Title of publication: 2,3-Dicyclohexylsuccinimide as a directing/protecting group for the regioselective glycosylation or alkylation of purines
• Authors of publication: Ayan Pal; Kerry J. Salandria; Joseph W. Arico; Mark K. Schlegel; Larry W. McLaughlin
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 2936
• a: 9.1585 ± 0.0013 Å
• b: 28.601 ± 0.004 Å
• c: 10.3611 ± 0.0015 Å
• α: 90°
• β: 92.664 ± 0.007°
• γ: 90°
• Cell volume: 2711.1 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0417
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.0937
• Weighted residual factors for all reflections included in the refinement: 0.0961
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No