Information card for entry 7109052

Structure parameters

• Chemical name: P-triphenyl-P'-2-pyridyl-diphenyl-carbodiphorphorane
• Formula: C79 H66 N2 P4
• Calculated formula: C79 H66 N2 P4
• Title of publication: Chiral heterobimetallic complexes of carbodiphosphoranes and phosphinidene_carbene adducts
• Authors of publication: Manuel Alcarazo; Karin Radkowski; Gerlinde Mehler; Richard Goddard; Alois Furstner
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 3140
• a: 10.5881 ± 0.0012 Å
• b: 11.7546 ± 0.0014 Å
• c: 13.4581 ± 0.0016 Å
• α: 73.849 ± 0.002°
• β: 73.626 ± 0.002°
• γ: 78.953 ± 0.002°
• Cell volume: 1531.9 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0856
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.1341
• Weighted residual factors for all reflections included in the refinement: 0.1524
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No