Information card for entry 7109095

Structure parameters

• Chemical name: [{Yb(NacNac)(Fp)(THF)}2(u-YbFp2)].1.5(C5H12)
• Formula: C101.5 H136 Fe4 N4 O10 Yb3
• Calculated formula: C101.5 H136 Fe4 N4 O10 Yb3
• Title of publication: Synthesis and reactions of beta-diketiminate-supported complexes with Mg-Fe or Yb-Fe bonds
• Authors of publication: Matthew P. Blake; Nikolas Kaltsoyannis; Philip Mountford
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 3315
• a: 13.3848 ± 0.0003 Å
• b: 17.1457 ± 0.0003 Å
• c: 24.9082 ± 0.0005 Å
• α: 98.5709 ± 0.0016°
• β: 94.0808 ± 0.0016°
• γ: 106.447 ± 0.0017°
• Cell volume: 5382.2 ± 0.2 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0434
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for all reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.0448
• Weighted residual factors for all reflections included in the refinement: 0.044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1024
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No