Crystallography Open Database

Information card for entry 7109109

Preview

Coordinates	7109109.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34.19 H41.46 F4 N2.7 O0.79 P Pt
Calculated formula	C34.188 H41.461 F4 N2.701 O0.786 P Pt
Title of publication	Unprecedented 1,3-migration of the aryl ligand in metallacyclic aryl alpha-naphthyl Pt(IV) difluorides to produce beta-arylnaphthyl Pt(II) complexes
Authors of publication	Ina S. Dubinsky-Davidchik; Israel Goldberg; Arkadi Vigalok; Andrei N. Vedernikov
Journal of publication	Chem.Commun.
Year of publication	2013
Journal volume	49
Pages of publication	3446
a	10.1311 ± 0.0003 Å
b	11.4959 ± 0.0004 Å
c	15.7724 ± 0.0005 Å
α	75.0835 ± 0.0016°
β	79.7841 ± 0.0018°
γ	86.3353 ± 0.0011°
Cell volume	1746.59 ± 0.1 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0751
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.1187
Weighted residual factors for all reflections included in the refinement	0.1301
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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