Information card for entry 7109377

Structure parameters

• Formula: C39 H59 N4 O Se Si
• Calculated formula: C39 H59 N4 O Se Si
• Title of publication: From elusive thio- and selenosilanoic acids to copper(I) complexes with intermolecular Si[double bond,length as m-dash]E > Cu-O-Si coordination modes(E=S,Se)
• Authors of publication: Gengwen Tan; Yun Xiong; Shigeyoshi Inoue; Stephan Enthaler; Burgert Blom; Jan D. Epping; Matthias Driess
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 5595
• a: 10.6226 ± 0.0007 Å
• b: 13.2004 ± 0.0007 Å
• c: 14.9165 ± 0.0008 Å
• α: 76.004 ± 0.004°
• β: 75.594 ± 0.005°
• γ: 73.587 ± 0.005°
• Cell volume: 1909.9 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0755
• Weighted residual factors for all reflections included in the refinement: 0.0788
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No