Information card for entry 7109379

Structure parameters

• Formula: C14 H23 Cl2 O Rh
• Calculated formula: C14 H23 Cl2 O Rh
• Title of publication: A robust method to heterogenise and recycle group 9 catalysts
• Authors of publication: Stephanie J. Lucas; Benjamin D. Crossley; Alan J. Pettman; Antony D. Vassileiou; Thomas E. O. Screen; A. John Blacker; Patrick C. McGowan
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 5562
• a: 12.7608 ± 0.0018 Å
• b: 9.1868 ± 0.0015 Å
• c: 13.945 ± 0.002 Å
• α: 90°
• β: 97.291 ± 0.01°
• γ: 90°
• Cell volume: 1621.6 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1717
• Residual factor for significantly intense reflections: 0.1103
• Weighted residual factors for significantly intense reflections: 0.2833
• Weighted residual factors for all reflections included in the refinement: 0.3301
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No