Information card for entry 7109624

Structure parameters

• Formula: C60 H98 P4 Sn2
• Calculated formula: C60 H98 P4 Sn2
• Title of publication: 1,2,3,4-Tetramesityl-1,4-bis(tri-n-butyltin)tetraphosphane: synthesis and molecular structure
• Authors of publication: Ivana Jevtovikj; Peter Lonnecke; Evamarie Hey-Hawkins
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 7355
• a: 9.543 ± 0.0002 Å
• b: 13.0225 ± 0.0004 Å
• c: 14.6643 ± 0.0004 Å
• α: 110.296 ± 0.002°
• β: 99.499 ± 0.002°
• γ: 106.251 ± 0.002°
• Cell volume: 1569.89 ± 0.08 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0349
• Residual factor for significantly intense reflections: 0.0259
• Weighted residual factors for significantly intense reflections: 0.0651
• Weighted residual factors for all reflections included in the refinement: 0.0671
• Goodness-of-fit parameter for all reflections included in the refinement: 0.993
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No