Information card for entry 7109686

Structure parameters

• Formula: C44 H42 Cl2 Co N12 Ni O Rh
• Calculated formula: C44 H42 Cl2 Co N12 Ni O Rh
• Title of publication: Facile synthesis of heterotrimetallic metal-string complex [NiCoRh(dpa)4Cl2] through direct metal replacement
• Authors of publication: Ming-Chuan Cheng; Chi-Lun Mai; Chen-Yu Yeh; Gene-Hsiang Lee; Shie-Ming Peng
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 7938
• a: 16.0264 ± 0.0002 Å
• b: 15.7368 ± 0.0003 Å
• c: 16.9707 ± 0.0002 Å
• α: 90°
• β: 99.9708 ± 0.0009°
• γ: 90°
• Cell volume: 4215.44 ± 0.11 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0718
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1016
• Weighted residual factors for all reflections included in the refinement: 0.1134
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No