Crystallography Open Database

Information card for entry 7109817

Preview

Coordinates	7109817.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H30 O8
Calculated formula	C22 H30 O8
Title of publication	Dimerization of cyclopropenes to bifurans using tandem metal relay catalysis
Authors of publication	Chuanling Song; Di Sun; Xianglong Peng; Jing Bai; Rongyi Zhang; Shengzhen Hou; Jianwu Wang; Zhenghu Xu
Journal of publication	Chem.Commun.
Year of publication	2013
Journal volume	49
Pages of publication	9167
a	22.579 ± 0.007 Å
b	4.8945 ± 0.0014 Å
c	22.195 ± 0.007 Å
α	90°
β	110.56 ± 0.004°
γ	90°
Cell volume	2296.6 ± 1.2 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	3
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0749
Residual factor for significantly intense reflections	0.0431
Weighted residual factors for significantly intense reflections	0.1049
Weighted residual factors for all reflections included in the refinement	0.1232
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7109817.html