Crystallography Open Database

Information card for entry 7109851

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Coordinates	7109851.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H29 N O S
Calculated formula	C19 H29 N O S
Title of publication	Highly diastereoselective radical cyclisations of chiral sulfinimines
Authors of publication	Elise M. Rochette; William Lewis; Al G. Dossetter; Robert A. Stockman
Journal of publication	Chem.Commun.
Year of publication	2013
Journal volume	49
Pages of publication	9395
a	20.64863 ± 0.00014 Å
b	20.64863 ± 0.00014 Å
c	11.2327 ± 0.0001 Å
α	90°
β	90°
γ	120°
Cell volume	4147.6 ± 0.05 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	5
Space group number	144
Hermann-Mauguin space group symbol	P 31
Hall space group symbol	P 31
Residual factor for all reflections	0.0453
Residual factor for significantly intense reflections	0.0432
Weighted residual factors for significantly intense reflections	0.122
Weighted residual factors for all reflections included in the refinement	0.1251
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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