Information card for entry 7110124

Structure parameters

• Formula: C33 H45 I N2 O2 S Sn
• Calculated formula: C33 H45 I N2 O2 S Sn
• Title of publication: Silver-catalyzed cascade cyclization-stannylation of o-alkynylaniline derivatives with 2-tributylstannylfuran: an efficient synthesis of (3-indolyl)stannanes
• Authors of publication: Jun Liu; Xin Xie; Yuanhong Liu
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 50
• Pages of publication: 11794
• a: 37.522 ± 0.003 Å
• b: 11.2412 ± 0.001 Å
• c: 18.3416 ± 0.0015 Å
• α: 90°
• β: 114.579 ± 0.002°
• γ: 90°
• Cell volume: 7035.3 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0665
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for significantly intense reflections: 0.1051
• Weighted residual factors for all reflections included in the refinement: 0.1184
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No