Information card for entry 7110142

Structure parameters

• Formula: C19 H30 O4 Si
• Calculated formula: C19 H30 O4 Si
• Title of publication: Desymmetrization of cyclic olefins via asymmetric Heck reaction and hydroarylation
• Authors of publication: Sijia Liu; Jianrong (Steve) Zhou
• Journal of publication: Chem.Commun.
• Year of publication: 2013
• Journal volume: 49
• Pages of publication: 11758
• a: 5.9056 ± 0.0005 Å
• b: 12.2286 ± 0.0012 Å
• c: 26.909 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1943.3 ± 0.3 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1183
• Residual factor for significantly intense reflections: 0.0791
• Weighted residual factors for significantly intense reflections: 0.1827
• Weighted residual factors for all reflections included in the refinement: 0.2096
• Goodness-of-fit parameter for all reflections included in the refinement: 1.14
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No