Crystallography Open Database

Information card for entry 7110166

Preview

Coordinates	7110166.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H80 Ag3 Cl4 F9 N4 O9 P4 S3
Calculated formula	C43 H80 Ag3 Cl4 F9 N4 O9 P4 S3
Title of publication	A novel, rigid diphosphine with an active NHC spacer; di- and trinuclear complexes of d10 coinage metals
Authors of publication	Pengfei Ai; Andreas A. Danopoulos; Pierre Braunstein; Kirill Yu. Monakhovc
Journal of publication	Chem.Commun.
Year of publication	2013
Journal volume	50
Pages of publication	103
a	16.5334 ± 0.0006 Å
b	15.6264 ± 0.0005 Å
c	25.5667 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	6605.3 ± 0.4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	9
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0973
Residual factor for significantly intense reflections	0.0454
Weighted residual factors for significantly intense reflections	0.0904
Weighted residual factors for all reflections included in the refinement	0.1137
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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