Information card for entry 7110248

Structure parameters

• Common name: tetramethylammonium pentaniobotellurate hydrate
• Formula: C20 H94 N5 Nb5 O39.25 Te
• Calculated formula: C20 H94 N5 Nb5.046 O39.29 Te0.954
• Title of publication: A tellurium-substituted Lindqvist-type polyoxoniobate showing high H2 evolution catalyzed by tellurium nanowires via photodecomposition
• Authors of publication: Jung-Ho Son; Jiarui Wang; Frank E. Osterloh; Ping Yu; William H. Casey
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 836
• a: 33.87 ± 0.0015 Å
• b: 8.4954 ± 0.0004 Å
• c: 21.9238 ± 0.001 Å
• α: 90°
• β: 110.475 ± 0.001°
• γ: 90°
• Cell volume: 5909.8 ± 0.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.019
• Residual factor for significantly intense reflections: 0.0163
• Weighted residual factors for significantly intense reflections: 0.0397
• Weighted residual factors for all reflections included in the refinement: 0.0407
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No