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Information card for entry 7110254
Preview
Coordinates | 7110254.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C81 H70 B2 Cl2 F8 P4 Pd2 |
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Calculated formula | C80 H68 B2 F8 P4 Pd2 |
SMILES | [B](F)(F)(F)[F-].[CH]12[CH]3=[CH](C=C[CH]4=[CH]5[CH]=2[Pd]45([P](c2ccccc2)(c2ccccc2)c2ccccc2)[P](c2ccccc2)(c2ccccc2)c2ccccc2)[Pd]13([P](c1ccccc1)(c1ccccc1)c1ccccc1)[P](c1ccccc1)(c1ccccc1)c1ccccc1.[B](F)(F)(F)[F-] |
Title of publication | Bis-cyclooctatetraene tripalladium sandwich complexes |
Authors of publication | Tetsuro Murahashi; Seita Kimura; Kohei Takase; Tomohito Uemura; Sensuke Ogoshi; Koji Yamamoto |
Journal of publication | Chem.Commun. |
Year of publication | 2014 |
Journal volume | 50 |
Pages of publication | 820 |
a | 25.3856 ± 0.0012 Å |
b | 24.7751 ± 0.001 Å |
c | 11.8833 ± 0.0006 Å |
α | 90° |
β | 93.678 ± 0.001° |
γ | 90° |
Cell volume | 7458.4 ± 0.6 Å3 |
Cell temperature | 123 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 7 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.1153 |
Residual factor for significantly intense reflections | 0.0727 |
Weighted residual factors for significantly intense reflections | 0.2067 |
Weighted residual factors for all reflections included in the refinement | 0.2643 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.913 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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