Information card for entry 7110347

Structure parameters

• Formula: C28.5 H24 Co F4 P
• Calculated formula: C28.5 H24 Co F4 P
• Title of publication: Stepwise addition of difluorocarbene to a transition metal centre
• Authors of publication: Graham M. Lee; Daniel J. Harrison; Ilia Korobkov; R. Tom Baker
• Journal of publication: Chem.Commun.
• Year of publication: 2014
• Journal volume: 50
• Pages of publication: 1128
• a: 8.9032 ± 0.0003 Å
• b: 9.6331 ± 0.0003 Å
• c: 15.0734 ± 0.0005 Å
• α: 98.01 ± 0.002°
• β: 95.934 ± 0.002°
• γ: 109.836 ± 0.002°
• Cell volume: 1188.35 ± 0.07 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0572
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1405
• Weighted residual factors for all reflections included in the refinement: 0.1474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No