Information card for entry 7110356

Structure parameters

• Common name: none
• Formula: C13 H17 K9 N12 Nb4 O13 Te4
• Calculated formula: C13 K9 N12 Nb4 O13 Te4
• Title of publication: Synthesis and structure of a tetranuclear niobium telluride cuboidal cluster with a central μ4-O ligand
• Authors of publication: Fedin, Vladimir P.; Kalinina, Irina V.; Virovets, Alexander V.; Podberezskaya, Nina V.; Neretin, Ivan S.; Slovokhotov, Yuri L.
• Journal of publication: Chemical Communications
• Year of publication: 1998
• Journal issue: 23
• Pages of publication: 2579
• a: 12.4688 ± 0.0009 Å
• b: 22.658 ± 0.004 Å
• c: 16.318 ± 0.002 Å
• α: 90°
• β: 91.584 ± 0.009°
• γ: 90°
• Cell volume: 4608.4 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for significantly intense reflections: 0.1151
• Weighted residual factors for all reflections included in the refinement: 0.1347
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No