Information card for entry 7110359

Structure parameters

• Formula: C47.5 H59 Cl7 Ge2 O4
• Calculated formula: C47.5 H59 Cl7 Ge2 O4
• Title of publication: Binuclear tin and germanium calix[4]arenes
• Authors of publication: McBurnett, Brian G.; Cowley, Alan H.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 1
• Pages of publication: 17
• a: 13.201 ± 0.002 Å
• b: 14.188 ± 0.002 Å
• c: 15.212 ± 0.002 Å
• α: 84.63 ± 0.01°
• β: 73.46 ± 0.01°
• γ: 64.98 ± 0.01°
• Cell volume: 2473.8 ± 0.7 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1679
• Residual factor for significantly intense reflections: 0.086
• Weighted residual factors for all reflections: 0.2629
• Weighted residual factors for significantly intense reflections: 0.2114
• Goodness-of-fit parameter for all reflections: 0.959
• Goodness-of-fit parameter for significantly intense reflections: 1.14
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No