Information card for entry 7110392

Structure parameters

• Formula: C12 H39 Ga3 O9
• Calculated formula: C14 H40 Ga3 O9
• Title of publication: Hydrogen bonded assemblies of a cyclic trimeric hydroxy gallium(III) derivative: [{Me2Ga(μ-OH)}3·3H2O]2·18-crown-6
• Authors of publication: Croucher, Paul D.; Drljaca, Alexander; Papadopoulos, Stavroula; Raston, Colin L.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 2
• Pages of publication: 153
• a: 8.9725 ± 0.0003 Å
• b: 11.312 ± 0.0003 Å
• c: 12.8986 ± 0.0005 Å
• α: 77.522 ± 0.001°
• β: 75.876 ± 0.001°
• γ: 67.686 ± 0.001°
• Cell volume: 1163.35 ± 0.07 ų
• Cell temperature: 273.2 K
• Ambient diffraction temperature: 273.2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.059
• Residual factor for significantly intense reflections: 0.031
• Weighted residual factors for all reflections: 0.0338
• Weighted residual factors for all reflections included in the refinement: 0.031
• Goodness-of-fit parameter for all reflections: 1.682
• Goodness-of-fit parameter for all reflections included in the refinement: 1.87
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No