Information card for entry 7110408

Structure parameters

• Formula: C38 H30 Cu N10 P2
• Calculated formula: C38 H30 Cu N10 P2
• Title of publication: Synthesis of the sodium diphenylbis(cyanamido)phosphonium diylide by a new variation of the Staudinger reaction
• Authors of publication: Taillefer, Marc; Inguimbert, Nicolas; Cristau, Henri-Jean; Jäger, Lothar; Merzweiler, Kurt
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 6
• Pages of publication: 565
• a: 8.4325 ± 0.0014 Å
• b: 13.5423 ± 0.0012 Å
• c: 16.555 ± 0.002 Å
• α: 107.588 ± 0.008°
• β: 91.823 ± 0.011°
• γ: 98.651 ± 0.011°
• Cell volume: 1775.6 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0739
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for all reflections: 0.133
• Weighted residual factors for significantly intense reflections: 0.1186
• Goodness-of-fit parameter for all reflections: 1.037
• Goodness-of-fit parameter for significantly intense reflections: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No