Information card for entry 7110420

Structure parameters

• Formula: C156 H182 Cu4 F24 N16 O3 P4
• Calculated formula: C156 H182 Cu4 F24 N16 O3 P4
• Title of publication: Chiral 1,2-ethanediyl-spaced quaterpyridines give a library of cyclic and double helicates with copper(I)
• Authors of publication: Constable, Edwin C.; Housecroft, Catherine E.; Kulke, Torsten; Baum, Gerhard; Fenske, Dieter
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 2
• Pages of publication: 195
• a: 12.576 ± 0.003 Å
• b: 16.179 ± 0.003 Å
• c: 21.058 ± 0.004 Å
• α: 96.86 ± 0.03°
• β: 95.34 ± 0.03°
• γ: 111 ± 0.03°
• Cell volume: 3928.5 ± 1.7 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 200 ± 1 K
• Number of distinct elements: 7
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.0565
• Weighted residual factors for all reflections: 0.1637
• Weighted residual factors for significantly intense reflections: 0.152
• Goodness-of-fit parameter for all reflections: 1.288
• Goodness-of-fit parameter for significantly intense reflections: 1.292
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No