Information card for entry 7110426

Structure parameters

• Formula: C19 H22 B Cl Fe Sn
• Calculated formula: C19 H22 B Cl Fe Sn
• Title of publication: Selective synthesis of 1-stanna-2-boraferrocenes: novel bidentate Lewis acids via an unexpected rearrangement reaction
• Authors of publication: Jäkle, Frieder; Lough, Alan J.; Manners, Ian
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 5
• Pages of publication: 453
• a: 11.0509 ± 0.0004 Å
• b: 14.1655 ± 0.0007 Å
• c: 11.7913 ± 0.0005 Å
• α: 90°
• β: 95.826 ± 0.003°
• γ: 90°
• Cell volume: 1836.29 ± 0.14 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0383
• Residual factor for significantly intense reflections: 0.0307
• Weighted residual factors for significantly intense reflections: 0.0786
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No