Information card for entry 7110492

Structure parameters

• Formula: C34 H88 As2 K2 N10 P2
• Calculated formula: C34 H88 As2 K2 N10 P2
• SMILES: [K]1234([N](C)(C)CC[N]1(C)CC[N]2(C)C)[N](C)(C)[As](N(C)C)[P]3(C(C)(C)C)[K]123([N](C)(C)CC[N]1(C)CC[N]2(C)C)[N](C)(C)[As](N(C)C)[P]34C(C)(C)C
• Title of publication: A simple route to multifunctional phosphide and amide donor sets; syntheses and structures of [{ButPAs(NMe2)2}K.pmdeta]2 and [{CyNAs(NMe2)2K}2]\ιnfty
• Authors of publication: Beswick, Michael A.; Hopkins, Alexander D.; Kidd, Sara J.; Lawson, Yvonne G.; Raithby, Paul R.; Wright, Dominic S.; Bashall, Alan; McPartlin, Mary; Rothenberger, Alexander; Stalke, FT3Dietmar
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 8
• Pages of publication: 739
• a: 14.014 ± 0.003 Å
• b: 12.75 ± 0.003 Å
• c: 15.014 ± 0.003 Å
• α: 90°
• β: 105.48 ± 0.03°
• γ: 90°
• Cell volume: 2585.4 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1468
• Residual factor for significantly intense reflections: 0.0733
• Weighted residual factors for significantly intense reflections: 0.1536
• Weighted residual factors for all reflections included in the refinement: 0.1854
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No