Information card for entry 7110515
Formula
C29 H28 O S3
Calculated formula
C29 H28 O S3
Title of publication
Formation of 2-oxa- or 2-azabicyclo[3.3.0]octa-3,7-diene by a novel tandem intramolecular photo-cyclization of 2,4,6-tris(phenylthio)hepta-2,4,6-trienal derivatives
Authors of publication
Yoshimatsu, Mitsuhiro; Gotoh, Satoshi; Tanabe, Genzoh; Muraoka, Osamu
Journal of publication
Chemical Communications
Year of publication
1999
Journal issue
10
Pages of publication
909
a
9.007 ± 0.002 Å
b
26.879 ± 0.006 Å
c
10.945 ± 0.002 Å
α
90.02 ± 0.02°
β
99.34 ± 0.02°
γ
89.99 ± 0.02°
Cell volume
2614.6 ± 1 Å3
Cell temperature
298 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for significantly intense reflections
0.056
Weighted residual factors for significantly intense reflections
0.07
Goodness-of-fit parameter for significantly intense reflections
3.28
Diffraction radiation wavelength
1.54178 Å
Diffraction radiation type
CuIKa
Has coordinates
Yes
Has disorder
No
Has Fobs
No
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https://www.crystallography.net/7110515.html