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Information card for entry 7110518
Preview
Coordinates | 7110518.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | bis(R,R)-(-)-trans-2,3-bis(diphenylhydroxymethyl)-1,4-dioxaspiro(4.4)nonane N-nitroso-4-phenylpiperidine clathrate |
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Formula | C44 H46 N2 O5 |
Calculated formula | C44 H46 N2 O5 |
Title of publication | N-Nitrosopiperidines with chirality solely due to hindered rotation about the N‒N bond: enantioselective inclusion complexation with optically active hosts |
Authors of publication | Olszewska, Teresa; Milewska, Maria J.; Połoński, Tadeusz; Gdaniec, Maria |
Journal of publication | Chemical Communications |
Year of publication | 1999 |
Journal issue | 15 |
Pages of publication | 1385 |
a | 11.292 ± 0.002 Å |
b | 9.536 ± 0.002 Å |
c | 17.654 ± 0.004 Å |
α | 90° |
β | 97.04 ± 0.02° |
γ | 90° |
Cell volume | 1886.7 ± 0.7 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0696 |
Residual factor for significantly intense reflections | 0.0418 |
Weighted residual factors for all reflections | 0.1271 |
Weighted residual factors for significantly intense reflections | 0.1108 |
Goodness-of-fit parameter for all reflections | 1.072 |
Goodness-of-fit parameter for significantly intense reflections | 1.126 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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