The first organoelement oxides containing three different metals; synthesis and structure of (Ph2SiOR2SnOMO) [R = (CH2)3NMe2; M = But2Sn, But2Ge, PhB]† ‡
Authors of publication
Beckmann, Jens; Jurkschat, Klaus; Pieper, Nicole; Schürmann, Markus
Journal of publication
Chemical Communications
Year of publication
1999
Journal issue
12
Pages of publication
1095
a
10.63 ± 0.001 Å
b
17.201 ± 0.001 Å
c
17.3 ± 0.001 Å
α
100.001 ± 0.001°
β
90.737 ± 0.001°
γ
104.343 ± 0.001°
Cell volume
3012.9 ± 0.4 Å3
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0521
Residual factor for significantly intense reflections
0.0311
Weighted residual factors for significantly intense reflections
0.0735
Weighted residual factors for all reflections included in the refinement
0.0796
Goodness-of-fit parameter for all reflections included in the refinement