Information card for entry 7110551

Structure parameters

• Formula: C24 H27 Cl5 F12 O6 P2 Pd
• Calculated formula: C24 H27 Cl5 F12 O6 P2 Pd
• Title of publication: Bis(phospha-adamantyl)alkanes: a new class of very bulky diphosphines
• Authors of publication: Gee, Victoria; Guy Orpen, A.; Phetmung, Hirihattaya; Pringle, Paul G.; Pugh, Robert I.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 10
• Pages of publication: 901
• a: 13.142 ± 0.002 Å
• b: 11.987 ± 0.002 Å
• c: 22.167 ± 0.003 Å
• α: 90°
• β: 102.419 ± 0.008°
• γ: 90°
• Cell volume: 3410.3 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0304
• Residual factor for significantly intense reflections: 0.0251
• Weighted residual factors for all reflections: 0.0656
• Weighted residual factors for significantly intense reflections: 0.0558
• Goodness-of-fit parameter for all reflections: 0.885
• Goodness-of-fit parameter for significantly intense reflections: 0.906
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No