Information card for entry 7110585

Structure parameters

• Common name: [PtCl(PMe3)(C15H32O3P3)].2.5(CH2Cl2)
• Formula: C20.5 H46 Cl6 O3 P4 Pt
• Calculated formula: C20.5 H47 Cl6 O3 P4 Pt
• Title of publication: First η1-ligated 2,4,6-tri-tert-butyl-1,3,5-triphosphabenzene complexes and the remarkable trihydration reaction of trans-[PtCl2(PMe3)(P3C3But3)] to cis-[PtCl(PMe3)(P3O3C3H5But3)], containing the novel CH(But)PH(O)C(But)PH(O)CH(But)P(O) ring system
• Authors of publication: Clendenning, Scott B.; Hitchcock, Peter B.; Nixon, John F.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 15
• Pages of publication: 1377
• a: 14.508 ± 0.009 Å
• b: 15.924 ± 0.009 Å
• c: 29.018 ± 0.012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6704 ± 6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 64
• Hermann-Mauguin space group symbol: C m c a
• Hall space group symbol: -C 2ac 2
• Residual factor for all reflections: 0.0921
• Residual factor for significantly intense reflections: 0.0746
• Weighted residual factors for significantly intense reflections: 0.1957
• Weighted residual factors for all reflections included in the refinement: 0.2088
• Goodness-of-fit parameter for all reflections included in the refinement: 1.12
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No