Information card for entry 7110589

Structure parameters

• Formula: C36 H82 Mg2 N2 O4 Si4
• Calculated formula: C36 H74.2 Mg2 N2 O4 Si4
• Title of publication: Bis(amido)magnesium mediated aldol additions: first structural characterisation of an amidomagnesium aldolate intermediate
• Authors of publication: Allan, John F.; Henderson, Kenneth W.; Kennedy, Alan R.
• Journal of publication: Chemical Communications
• Year of publication: 1999
• Journal issue: 14
• Pages of publication: 1325
• a: 9.61 ± 0.003 Å
• b: 11.381 ± 0.002 Å
• c: 12.024 ± 0.004 Å
• α: 98.9 ± 0.02°
• β: 104 ± 0.02°
• γ: 105.996 ± 0.019°
• Cell volume: 1191.6 ± 0.6 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0661
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1337
• Weighted residual factors for all reflections included in the refinement: 0.1417
• Goodness-of-fit parameter for all reflections included in the refinement: 1.138
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No