Information card for entry 7110810

Structure parameters

• Formula: C80 H60 Ag2 B2 Cl1.5 F8 N1.5 O3 P6
• Calculated formula: C79.99 H60 Ag2 B1.998 Cl1.5 F8 N1.49 O2.98 P6
• Title of publication: Triply-bridged diphos disilver helical complexes [Ag2(μ2-dppa-P,P′)3(anion)2] [dppa = bis(diphenylphosphino)acetylene]
• Authors of publication: James, Stuart L.; Lozano, Elvira; Nieuwenhuyzen, Mark
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 7
• Pages of publication: 617
• a: 22.1929 ± 0.0016 Å
• b: 14.8355 ± 0.0018 Å
• c: 23.8561 ± 0.0013 Å
• α: 90°
• β: 99.46 ± 0.006°
• γ: 90°
• Cell volume: 7747.6 ± 1.2 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0674
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.0963
• Weighted residual factors for all reflections included in the refinement: 0.1067
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No