Information card for entry 7110939

Structure parameters

• Formula: C18 H43 Cl P2 Ru
• Calculated formula: C18 H43 Cl P2 Ru
• Title of publication: A 14-electron ruthenium hydride: the key intermediate in the synthesis of ruthenium carbene complexes; X-ray structure of [RuHCl(PPri3)2]
• Authors of publication: van der Schaaf, Paul A.; Kolly, Roman; Hafner, Andreas
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 12
• Pages of publication: 1045
• a: 8.0682 ± 0.0005 Å
• b: 8.9506 ± 0.0008 Å
• c: 16.6435 ± 0.0012 Å
• α: 90°
• β: 92.763 ± 0.0009°
• γ: 90°
• Cell volume: 1200.52 ± 0.16 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.045
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.1168
• Weighted residual factors for all reflections included in the refinement: 0.1219
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No