Crystallography Open Database

Information card for entry 7110941

Preview

Structure parameters

Formula	C36 H67 Cl P2 Ru
Calculated formula	C36 H67 Cl P2 Ru
Title of publication	A 14-electron ruthenium hydride: the key intermediate in the synthesis of ruthenium carbene complexes; X-ray structure of [RuHCl(PPri3)2]
Authors of publication	van der Schaaf, Paul A.; Kolly, Roman; Hafner, Andreas
Journal of publication	Chemical Communications
Year of publication	2000
Journal issue	12
Pages of publication	1045
a	9.8438 ± 0.0008 Å
b	10.2011 ± 0.0008 Å
c	10.8356 ± 0.0009 Å
α	114.29 ± 0.009°
β	108.475 ± 0.009°
γ	90.824 ± 0.01°
Cell volume	927.37 ± 0.17 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0439
Residual factor for significantly intense reflections	0.0412
Weighted residual factors for significantly intense reflections	0.1251
Weighted residual factors for all reflections included in the refinement	0.1277
Goodness-of-fit parameter for all reflections included in the refinement	1.09
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7110941.html