Information card for entry 7110987

Structure parameters

• Formula: C29 H51 N3 Se W
• Calculated formula: C29 H51 N3 Se W
• Title of publication: Synthesis and structures of half-sandwich W(vi) tri(selenido) and W(ii) selenolato complexes
• Authors of publication: Kawaguchi, Hiroyuki; Tatsumi, Kazuyuki
• Journal of publication: Chemical Communications
• Year of publication: 2000
• Journal issue: 14
• Pages of publication: 1299
• a: 9.7349 ± 0.0008 Å
• b: 18.9776 ± 0.0005 Å
• c: 17.4477 ± 0.0003 Å
• α: 90°
• β: 97.1791 ± 0.0007°
• γ: 90°
• Cell volume: 3198.1 ± 0.3 ų
• Cell temperature: 273.2 K
• Ambient diffraction temperature: 273.2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0774
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.0597
• Weighted residual factors for all reflections included in the refinement: 0.0635
• Goodness-of-fit parameter for all reflections included in the refinement: 1.472
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No