1,3-Diphenyl-2,2,2,4,4,4-hexazido-1,3-diaza-2,4-diphosphetidine: synthesis and structural characterisation of the first nitrogen-penta-coordinated phosphorus with three azide-groups
Authors of publication
Aubauer, Christoph; Klapötke, Thomas M.; Nöth, Heinrich; Schulz, Axel; Suter, Max; Weigand, Jan
Journal of publication
Chemical Communications
Year of publication
2000
Journal issue
24
Pages of publication
2491
a
7.3415 ± 0.0015 Å
b
8.5508 ± 0.0018 Å
c
17.879 ± 0.004 Å
α
88.527 ± 0.003°
β
85.499 ± 0.004°
γ
67.684 ± 0.003°
Cell volume
1035.1 ± 0.4 Å3
Cell temperature
193 ± 2 K
Ambient diffraction temperature
193 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.092
Residual factor for significantly intense reflections
0.0488
Weighted residual factors for significantly intense reflections
0.1148
Weighted residual factors for all reflections included in the refinement
0.1273
Goodness-of-fit parameter for all reflections included in the refinement
