Information card for entry 7111134

Structure parameters

• Formula: C25 H41 Li N4
• Calculated formula: C25 H41 Li N4
• SMILES: N([C@@H](C)c1ccccc1)([Li]12[N](CC[N]2(C)C)(C)CC[N]1(C)C)[C@@H](C)c1ccccc1
• Title of publication: Crystal structures of (R,R)-{[Ph(Me)CH]2NLi·pmdeta} and {[PhC(CH2)NH]Na·pmdeta}2: alkali metal amides derived from (R,R)-bis(α-methylbenzyl)amine
• Authors of publication: Andrews, Philip C.; Duggan, Peter J.; Maguire, Melissa; Nichols, Peter J.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 1
• Pages of publication: 53
• a: 9.987 ± 0.002 Å
• b: 13.692 ± 0.003 Å
• c: 18.553 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2537 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1771
• Residual factor for significantly intense reflections: 0.0911
• Weighted residual factors for significantly intense reflections: 0.1261
• Weighted residual factors for all reflections included in the refinement: 0.1509
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No