Information card for entry 7111164

Structure parameters

• Formula: C27 H63 N6 O P Si Sn8
• Calculated formula: C27 H66 N6 O P Si Sn8
• Title of publication: Synthesis and structure of [{Sn4(NBut)3P}{Sn4(NBut)3(OSiMe3)}]; a low-oxidation state p-block metal complex containing a P3− anion
• Authors of publication: Mosquera, Marta E. G.; Hopkins, Alexander D.; Raithby, Paul R.; Rothenberger, Alexander; Woods, Anthony D.; Wright, Dominic S.; Steiner, Alexander
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 4
• Pages of publication: 327
• a: 13.453 ± 0.003 Å
• b: 15.28 ± 0.003 Å
• c: 12.736 ± 0.003 Å
• α: 90°
• β: 116 ± 0.03°
• γ: 90°
• Cell volume: 2353.1 ± 1.1 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 7
• Space group number: 8
• Hermann-Mauguin space group symbol: C 1 m 1
• Hall space group symbol: C -2y
• Residual factor for all reflections: 0.0593
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for all reflections: 0.1928
• Weighted residual factors for significantly intense reflections: 0.0875
• Goodness-of-fit parameter for all reflections: 1.056
• Goodness-of-fit parameter for significantly intense reflections: 1.082
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No