Information card for entry 7111237

Structure parameters

• Formula: C52 H48 N32 Ni4 O2
• Calculated formula: C52 H48 N32 Ni4 O2
• Title of publication: Synthesis, structure and magnetism of a new dicubane-like ferromagnetic tetranuclear nickel cluster containing versatile azido-only bridges and a bis(bidentate) Schiff base blockerElectronic supplementary information (ESI) available: a plot of the reduced magnetisation (M/N??) vs. H for 1 at 2 K. See http://www.rsc.org/suppdata/cc/b2/b205375f/
• Authors of publication: Karmakar, Tapan K.; Chandra, Swapan K.; Ribas, Joan; Mostafa, Golam; Lu, Tian H.; Ghosh, Barindra K.
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 20
• Pages of publication: 2364
• a: 12.9364 ± 0.0009 Å
• b: 17.77 ± 0.0013 Å
• c: 14.4261 ± 0.001 Å
• α: 90°
• β: 106.69 ± 0.002°
• γ: 90°
• Cell volume: 3176.6 ± 0.4 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0747
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.1445
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No