Information card for entry 7111252

Structure parameters

• Formula: C43 H37 Cl Fe O4 P2 Pd
• Calculated formula: C43 H37 Cl Fe O4 P2 Pd
• Title of publication: Facile axial chirality control by using a precursor with central chirality. Application to the preparation of new axially chiral diphosphine complexes for asymmetric catalysis
• Authors of publication: Lotz, Matthias; Kramer, Gernot; Knochel, Paul
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 2546
• a: 9.7463 ± 0.0001 Å
• b: 18.7721 ± 0.0002 Å
• c: 20.4955 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3749.83 ± 0.07 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.055
• Residual factor for significantly intense reflections: 0.04
• Weighted residual factors for significantly intense reflections: 0.1006
• Weighted residual factors for all reflections included in the refinement: 0.11
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No