Information card for entry 7111254

Structure parameters

• Chemical name: [Pb(timpt)(NO3)](NO3)-0.417(Et2O)-0.167(H2O)
• Formula: C34.67 H31.5 N11 O6.58 Pb
• Calculated formula: C34.666 H31.165 N11 O6.5835 Pb
• Title of publication: 2D 4.82 Network with threefold parallel interpenetration from nanometer-sized tripodal ligand and lead(ii) nitrateElectronic supplementary information available: Fig. 1S. See http://www.rsc.org/suppdata/cc/b2/b207568g/
• Authors of publication: Wan, Shuang-Yi; Fan, Jian; Okamura, Taka-aki; Zhu, Hui-Fang; Ouyang, Xing-Mei; Sun, Wei-Yin; Ueyama, Norikazu
• Journal of publication: Chemical Communications
• Year of publication: 2002
• Journal issue: 21
• Pages of publication: 2520
• a: 33.6859 ± 0.0007 Å
• b: 7.7447 ± 0.0002 Å
• c: 30.8578 ± 0.001 Å
• α: 90°
• β: 116.014 ± 0.0011°
• γ: 90°
• Cell volume: 7234.8 ± 0.3 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1504
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.0871
• Weighted residual factors for all reflections included in the refinement: 0.1027
• Goodness-of-fit parameter for all reflections included in the refinement: 0.887
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No