Information card for entry 7111300

Structure parameters

• Formula: C52 H54 B2 Li4 N4 O7
• Calculated formula: C52 H54 B2 Li4 N4 O7
• Title of publication: Heterobimetallic lithium alkyltriimido aluminate cages containing the [R?Al(NR)3]4? tetraanion (R? = Bun, Et; R = 2-OMeC6H4)Electronic supplementary information (ESI) available: syntheses of 1?4. See http://www.rsc.org/suppdata/cc/b3/b307589c/
• Authors of publication: Copsey, May C.; Jeffery, John C.; Russell, Christopher A.; Slattery, John M.; Straughan, Jennifer A.
• Journal of publication: Chemical Communications
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2356
• a: 16.98 ± 0.003 Å
• b: 14.215 ± 0.003 Å
• c: 21.294 ± 0.004 Å
• α: 90°
• β: 107.21 ± 0.03°
• γ: 90°
• Cell volume: 4909.6 ± 1.8 ų
• Cell temperature: 373 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0631
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for significantly intense reflections: 0.1459
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No