Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7111316
Preview
Coordinates | 7111316.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | (R)-N-(3-buthoxycarbonyl-1-isopropyl)-2,3:5,6-bis-O- isopropylidene-D-mannose-imine N-oxide |
---|---|
Formula | C23 H41 N O8 |
Calculated formula | C23 H41 N O8 |
Title of publication | Radical addition of nitrones to acrylates mediated by SmI2: asymmetric synthesis of ?-amino acids employing carbohydrate-based chiral auxiliariesElectronic Supplementary Information (ESI) available: crystallographic data of 2b and 4a, experimental procedure and spectral data. See http://www.rsc.org/suppdata/cc/b4/b405141f/ |
Authors of publication | Johannesen, Sine A.; Albu, Silvia; Hazell, Rita G.; Skrydstrup, Troels |
Journal of publication | Chemical Communications |
Year of publication | 2004 |
Journal issue | 17 |
Pages of publication | 1962 - 1963 |
a | 6.54 ± 0.007 Å |
b | 19.97 ± 0.02 Å |
c | 20 ± 0.02 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2612 ± 5 Å3 |
Cell temperature | 120 K |
Ambient diffraction temperature | 120 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for significantly intense reflections | 0.049 |
Weighted residual factors for all reflections included in the refinement | 0.047 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.235 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7111316.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.