Information card for entry 7111323

Structure parameters

• Formula: C52.5 H56.5 Cl10 N12 P4 Pd4
• Calculated formula: C52.5 H55.5 Cl10 N12 P4 Pd4
• Title of publication: Unprecedented eight-palladium(i) crown-cycle with metal?metal unsupported bonds
• Authors of publication: Angurell, Inma; Mart�nez-Ruiz, Isabel; Rossell, Oriol; Seco, Miquel; G�mez-Sal, Pilar; Mart�n, Avelino
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 15
• Pages of publication: 1712 - 1713
• a: 32.541 ± 0.011 Å
• b: 17.474 ± 0.004 Å
• c: 24.144 ± 0.002 Å
• α: 90°
• β: 101.257 ± 0.01°
• γ: 90°
• Cell volume: 13465 ± 6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.083
• Residual factor for significantly intense reflections: 0.0504
• Weighted residual factors for significantly intense reflections: 0.1191
• Weighted residual factors for all reflections included in the refinement: 0.1408
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No