Information card for entry 7111351

Structure parameters

• Formula: C76 H101 N O8 V2
• Calculated formula: C76 H101 N O8 V2
• Title of publication: Vanadyl complexes bearing bi- and triphenolate chelate ligands: highly active ethylene polymerisation procatalystsElectronic supplementary information (ESI) available: selected spectroscopic and polymerisation data. See http://www.rsc.org/suppdata/cc/b4/b406783e/
• Authors of publication: Redshaw, Carl; Warford, Lee; Dale, Sophie H.; Elsegood, Mark R. J.
• Journal of publication: Chemical Communications
• Year of publication: 2004
• Journal issue: 17
• Pages of publication: 1954 - 1955
• a: 18.2798 ± 0.0004 Å
• b: 18.2851 ± 0.0005 Å
• c: 22.6903 ± 0.0007 Å
• α: 82.991 ± 0.002°
• β: 73.067 ± 0.002°
• γ: 89.982 ± 0.002°
• Cell volume: 7196.2 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1585
• Residual factor for significantly intense reflections: 0.1097
• Weighted residual factors for significantly intense reflections: 0.2497
• Weighted residual factors for all reflections included in the refinement: 0.2733
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No